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1 article(s) from Kretschmer, Katja

Novel multi-responsive P2VP-block-PNIPAAm block copolymers via nitroxide-mediated radical polymerization

Cathrin Corten,
Katja Kretschmer and
Dirk Kuckling

Beilstein J. Org. Chem. 2010, 6, 756–765, doi:10.3762/bjoc.6.89

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Graphical Abstract

Scheme 1: Synthesis of the nitroxide-terminated P2VP-macroinitiator.

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Figure 1: Plots of ln(M₀/M_t) and molecular weight distribution vs time of the homopolymerization of 2VP at ■ ...

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Figure 2: Plots of number average molecular weight vs conversion for the homopolymerization of 2VP for ■ 90 °...

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Figure 3: Plot of number average molecular weight vs conversion for the homopolymerization of 2VP at 110 °C w...

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Figure 4: MALDI-TOF MS of P2VP obtained for polymerizations stopped after 2, 4, 6, and 8 h. The samples were ...

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Scheme 2: Degradation of nitroxide-terminated P2VP-macroinitiator by laser light irradiation.

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Figure 5: MALDI-TOF MS of P2VP obtained for polymerizations stopped after 2 h. The samples were prepared by t...

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Scheme 3: Synthesis of the bi-responsive block copolymers.

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Figure 6: SEC traces for P2VP-block-PNIPAAm (solid line) and P2VP macroinitiator (dashed line).

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Figure 7: Demonstration of the solution behavior. Polymers from left to right: P2VP, PNIPAAm, P(2VP)₈₅-block-...

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Figure 8: Titration of P2VP₁₀₅-block-PNIPAAm₃₃₂ (1g/L) in 0.02 N HCl with 0.1 N NaOH at room temperature.

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Figure 9: Hydrodynamic radius distribution of P(2VP)₁₀₅-b-P(NIPAAm)₃₃₂ at ○ pH 7, T = 20 °C and ● pH 2, T= 45...

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Full Research Paper

Published 20 Aug 2010

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